uni-leipzig-open-access/json/s00706-023-03053-8

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Hydrolysis of trimetaphosphimic acid leads to the formation of diimidotriphosphoric acid by ring opening. Single-crystal structure determination using synchrotron radiation revealed the oxonium salt of the latter acid with double stacks of rod-shaped anions along [001]. Anharmonic displacement parameters were used to model slight disorder of part of the anions. These are interconnected by hydrogen bonds within and between the stacks. Powder X-ray diffraction confirmed phase purity. At temperatures above 120\u00a0\u00b0C, diimidotriphosphoric acid decomposes into unknown crystalline compounds. It thus seems a promising precursor for the synthesis of oxonitridophosphates at moderate temperatures.<\/jats:p>\n                <jats:p><jats:bold>Graphical abstract<\/jats:bold><\/jats:p>","DOI":"10.1007\/s00706-023-03053-8","type":"journal-article","created":{"date-parts":[[2023,3,28]],"date-time":"2023-03-28T07:02:45Z","timestamp":1679986965000},"page":"325-330","update-policy":"http:\/\/dx.doi.org\/10.1007\/springer_crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Oxonium diimidotriphosphate from the hydrolysis of trimetaphosphimic acid"],"prefix":"10.1007","volume":"154","author":[{"given":"Daniel","family":"G\u00fcnther","sequence":"first","affiliation":[]},{"given":"Carsten","family":"Paulmann","sequence":"additional","affiliation":[]},{"ORCID":"http:\/\/orcid.org\/0000-0003-0149-7066","authenticated-orcid":false,"given":"Oliver","family":"Oeckler","sequence":"additional","affiliation":[]}],"member":"297","published-online":{"date-parts":[[2023,3,28]]},"reference":[{"key":"3053_CR1","first-page":"9432","volume":"138","author":"S Das","year":"2016","unstructured":"Das S, Liu L, Zheng Y, Alachraf MW, Thiel W, De Kanta C, List B (2016) J Am Chem Soc 138:9432","journal-title":"J Am Chem Soc"},{"key":"3053_CR2","doi-asserted-by":"publisher","first-page":"5247","DOI":"10.1016\/j.tet.2016.06.031","volume":"72","author":"SM Langdon","year":"2016","unstructured":"Langdon SM (2016) Tetrahedron 72:5247","journal-title":"Tetrahedron"},{"key":"3053_CR3","doi-asserted-by":"publisher","first-page":"30","DOI":"10.1002\/zfch.19780180118","volume":"18","author":"HA Lehman","year":"1978","unstructured":"Lehman HA, T\u00f6pelmann W, Weichold R (1978) Z Chem 18:30","journal-title":"Z Chem"},{"key":"3053_CR4","doi-asserted-by":"publisher","first-page":"1","DOI":"10.1002\/zaac.19754150102","volume":"415","author":"L Riesel","year":"1975","unstructured":"Riesel L, Somieski R (1975) Z Anorg Allg Chem 415:1","journal-title":"Z Anorg Allg Chem"},{"key":"3053_CR5","doi-asserted-by":"publisher","first-page":"246","DOI":"10.1002\/zaac.19754120308","volume":"412","author":"L Riesel","year":"1975","unstructured":"Riesel L, Somieski R (1975) Z Anorg Allg Chem 412:246","journal-title":"Z Anorg Allg Chem"},{"key":"3053_CR6","first-page":"3","volume":"258","author":"E Thilo","year":"1949","unstructured":"Thilo E, R\u00e4tz R (1949) Z Anorg Allg Chem 258:3","journal-title":"Z Anorg Allg Chem"},{"key":"3053_CR7","first-page":"1822","volume":"7","author":"W Wanek","year":"1967","unstructured":"Wanek W (1967) Z Chem 7:1822","journal-title":"Z Chem"},{"key":"3053_CR8","first-page":"2712","volume":"35","author":"W Wanek","year":"1969","unstructured":"Wanek W, Thilo E (1969) Chem Commun 35:2712","journal-title":"Chem Commun"},{"key":"3053_CR9","doi-asserted-by":"publisher","first-page":"139","DOI":"10.1002\/zaac.19764190207","volume":"419","author":"R Attig","year":"1976","unstructured":"Attig R, Mootz D (1976) Z Anorg Allg Chem 419:139","journal-title":"Z Anorg Allg Chem"},{"key":"3053_CR10","volume":"648","author":"D G\u00fcnther","year":"2022","unstructured":"G\u00fcnther D, Kalischer C, Oeckler O (2022) Z Anorg Allg Chem 648:e202200259","journal-title":"Z Anorg Allg Chem"},{"key":"3053_CR11","doi-asserted-by":"publisher","first-page":"525","DOI":"10.1107\/S0108270186095513","volume":"42","author":"WP Bosman","year":"1986","unstructured":"Bosman WP, Beureksen PT, Smits JMM, Behm H, Mintjens J, Meisel W, Fuggle JC (1986) Acta Crystallogr Sect C 42:525","journal-title":"Acta Crystallogr Sect C"},{"key":"3053_CR12","doi-asserted-by":"publisher","first-page":"1442","DOI":"10.1021\/ic00256a023","volume":"26","author":"R Pozas-Tormo","year":"1987","unstructured":"Pozas-Tormo R, Moreno-Real L, Martinez-Lara M, Bruque-Gamez S (1987) Inorg Chem 26:1442","journal-title":"Inorg Chem"},{"key":"3053_CR13","doi-asserted-by":"publisher","first-page":"159","DOI":"10.1039\/JM9950500159","volume":"5","author":"MJ Hodson","year":"1995","unstructured":"Hodson MJ, Locke W, Mitchel PCH (1995) J Mater Chem 5:159","journal-title":"J Mater Chem"},{"key":"3053_CR14","volume-title":"Phosphor(V)-oxidnitride: Von molekularen und molekularionischen Vorstufen zu kondensierten Festk\u00f6rpern","author":"N Stock","year":"1998","unstructured":"Stock N (1998) Phosphor(V)-oxidnitride: Von molekularen und molekularionischen Vorstufen zu kondensierten Festk\u00f6rpern. 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